DEFINITION :
A report is a news article or broadcast which gives information about something that has just happened. report Used to indicate that something has been stated, although one cannot confirm its accuracy.
STRUCTURE :
TITLE PAGE | report title your name submission date |
EXECUTIVE SUMMARY | overview of subject matter methods of analysis findings recommendations |
TABLE OF CONTENTS | list of numbered sections in report and their page numbers |
INTRODUCTION | terms of reference outline of report’s structure |
BODY | headings and sub-headings which reflect the contents of each section. Includes information on method of data collection (if applicable), the findings of the report and discussion of findings in light of theory |
CONCLUSION | states the major inferences that can be drawn from the discussion makes recommendations |
REFERENCE LIST | list of reference material consulted during research for report |
APPENDIX | information that supports your analysis but is not essential to its explanat LAB REPORT |
A lab report is how you explain what you did in your experiment, what you learned, and what the results meant. Here is a standard format. If you prefer, you can print and fill in the science lab report template or download the pdf version of the template.
Title Page
- Not all lab reports have title pages, but if your instructor wants one, it would be a single page that states:
- The title of the experiment.
- Your name and the names of any lab partners.
- Your instructor's name.
- The date the lab was performed or the date the report was submitted.
- Title
- The title says what you did. It should be brief (aim for ten words or less) and describe the main point of the experiment or investigation. An example of a title would be: "Effects of Ultraviolet Light on Borax Crystal Growth Rate". If you can, begin your title using a keyword rather than an article like 'The' or 'A'.
- Introduction / Purpose
- Usually, the Introduction is one paragraph that explains the objectives or purpose of the lab. In one sentence, state the hypothesis. Sometimes an introduction may contain background information, briefly summarize how the experiment was performed, state the findings of the experiment, and list the conclusions of the investigation.
- Materials
- List everything needed to complete your experiment.
- Methods
- Describe the steps you completed during your investigation. This is your procedure. Be sufficiently detailed that anyone could read this section and duplicate your experiment. Write it as if you were giving direction for someone else to do the lab. It may be helpful to provide a Figure to diagram your experimental .
- Data
- Numerical data obtained from your procedure usually is presented as a table. Data encompasses what you recorded when you conducted the experiment. It's just the facts, not any interpretation of what they mean.
- Results
- Describe in words what the data means. Sometimes the Results section is combined with the Discussion (Results & Discussion).
- Discussion or Analysis
- The Data section contains numbers. The Analysis section contains any calculations you made based on those numbers. This is where you interpret the data and determine whether or not a hypothesis was accepted.
- Conclusions
- Most of the time the conclusion is a single paragraph that sums up what happened in the experiment, whether your hypothesis was accepted or rejected, and what this means.
- Figures & Graphs
Graphs and figures must both be labeled with a descriptive title. Label the axes on a graph, being sure to include units of measurement.
- References
- If your research was based on someone else's work or if you cited facts that require documentation, then you should list these references.
"Identification of a Compound
using Melting and Boiling Points"
Time and place
Day / Date: Thursday / October 09, 2014
Time: 13.20-15.50 WIB
Place: Dasa Chemical Laboratory
Introduction
One of the primary methods used to characterize a new
compound is the physical determination of its normal melting and boiling points.
The “normal” melting and boiling point is the temperature at which a
substance melts or boils when the barometric pressure is 760 mmHg or 1 atm.
In this experiment we will first calibrate our thermometers using ice and
water, whose normal melting and boiling points are well characterized as 0.0 °C
and 100.0 °C,
respectively[1].
Following this, we will measure the normal melting and boiling points of
an unknown compound. We will use this data to determine the identity of our
unknown from a list of possible unknown samples and physical data from the Chemical
Handbook[2].
Experimental
Procedure
As described in the lab
manual,[3]
ice was placed in a beaker and warmed until approximately 50% had melted.
The temperature of the ice/water mixture was then measured with a
thermometer. This was followed by a similar measurement of our solid unknown.
In part II, water was heated until boiling and the temperature of the
liquid/gas mixture measured with a thermometer.
This was followed by a similar measurement using our unknown compound. To get the best results possible, the procedure in the manual
was modified by repeating each trial three times.
Data & Results
The Barometric pressure in the lab was
measured to be 761.2 mmHg.
Table One – Experimental Data
Trial
|
Water
Melting Pt.
|
Water
Boiling Pt.
|
Unknown 7
Melting Pt.
|
Unknown 7
Boiling Pt.
|
1
|
101.2 °C
|
80.2 °C
|
272.7 °C
|
|
2
|
0.1 °C
|
101.1 °C
|
80.7 °C
|
272.8 °C
|
3
|
0.0 °C
|
100.9 °C
|
80.4 °C
|
273.0 °C
|
4
|
0.1 °C
|
n/a
|
n/a
|
n/a
|
Averages:
|
0.15 °C
|
101.1 °C
|
80.4 °C
|
272.8
°C
|
Standard
deviation (s):
|
± 0.06
|
± 0.15
|
± 0.15
|
± 0.06
|
95%
confidence limits:
|
± 0.14
|
± 0.4
|
± 0.4
|
± 0.14
|
*
This trial was eliminated because the thermometer was broken (there was a bubble
of air in the mercury). A new
thermometer was obtained from the stockroom and used for all other data.
Observations: The unknown was yellowish-orange in color and had a fruity smell.
As can be seen from our water data the
experimental values for the melting and boiling points of water differed from
the theoretical values by +0.15 °C
and +1.1 °C,
respectively. These differences
were used to calibrate the average data for the unknown.
Thus the corrected values for the unknown boiling and melting points are
given in Table 2.
Table Two – Corrected Temperatures
Unknown 7
Melting Pt.
|
Unknown 7
Boiling Pt.
|
|
Measured value |
80.4 °C
±
0.4 (95%)
|
272.80 ± 0.14 °C
(95%)
|
Correction
|
+0.15 °C
|
+ 1.1 °C
|
Corrected
value
|
80.5 °C ±
0.4 (95%)
|
273.90 ±
0.14 °C
(95%)
|
These values were used to identify our
unknown. Table Three below lists
possible unknowns and the melting and boiling points for these compounds found
in the Chemical Handbook.2
Table Three – Reference Data from Chemical Handbook
Compound
|
Melting Point
|
Boiling Point
|
Blabber Gas |
-15.8 °C
|
17.2 °C
|
Freezer Gel
|
82.7 °C
|
456.1 °C
|
Silly Putty
|
57.2 °C
|
121 °C
|
Billgatesium
|
1000 °C
|
unknown
|
Farsel Juice
|
80.8 °C
|
274.0 °C
|
Shampoo
|
-1.2 °C
|
108.7 °C
|
Based on these data we conclude that our
sample was probably “Farsel Juice” since both the melting and boiling points
fall within the confidence limits of our average melting and boiling points.
Additional evidence to support our conclusion is that Farsel Juice is
described in the Chemical Handbook
as having a yellowish-orange in color and has a “peach-like” smell.
Our unknown was this color and one of our group members observed a
“fruity” smell when she opened the bottle.
Although our measured
melting and boiling points differed from the theoretical data by a few percent,
this difference was very small leading us to believe that our results were quite
good. While there is still room for
error in our results due to the change in boiling and melting points as a
function of atmospheric pressure this difference should be very small.
Other factors such as contaminates in the water used may have affected
the results, but again every effort to minimalize such effects was made by using
only deionized water. Finally we did encounter some problems with our thermometer
in the first trial, but this was fixed by replacing it at the stockroom.
Thus our careful work, our additional color and smell observations, and
the fact that the corrected average of data exactly matched only one of the
choices with 95% confidence, all suggest that our unknown was in fact Farsel
Juice.
Conclusions
In this lab we determined the identity
of our unknown to be Farsel Juice using normal melting and boiling points.
A future experiment might include an additional calibration using the
barometric pressure and/or inclusion of other chemical properties such as
reactions of the compounds with acids and stuff to further test the nature of
the chemicals and more positively identify the chemicals.
Bibliography
[1] Agenius, I.M., General
Chemistry for College, 2nd Ed., Overcharge Publishing House, Beverly
Hills California, 1999, page 12.
[2] Dr. Joe Scientist, Ed., Chemical
Handbook, 578th Ed., Big Chemical Press Inc., Bigtown, USA, 1999.
[3] Wizard, Mr., “Don’t
try this at home” – Experiments for General Chemistry, 1st Ed.,
Explosive Info Co., Ground Zero, 1978, Experiment 2, pp. 10-
document containing
information organized in a narrative, graphic, or tabular form, prepared
on ad hoc, periodic, recurring, regular, or as required basis. Reports
may refer to specific periods, events, occurrences, or subjects, and may
be communicated or presented in oral or written form.
2. To provide information.
Read more: http://www.businessdictionary.com/definition/report.html
2. To provide information.
Read more: http://www.businessdictionary.com/definition/report.html
document containing
information organized in a narrative, graphic, or tabular form, prepared
on ad hoc, periodic, recurring, regular, or as required basis. Reports
may refer to specific periods, events, occurrences, or subjects, and may
be communicated or presented in oral or written form.
2. To provide information.
Read more: http://www.businessdictionary.com/definition/report.html
2. To provide information.
Read more: http://www.businessdictionary.com/definition/report.html
A document containing
information organized in a narrative, graphic, or tabular form, prepared
on ad hoc, periodic, recurring, regular, or as required basis. Reports
may refer to specific periods, events, occurrences, or subjects, and may
be communicated or presented in oral or written form.
2. To provide information.
Read more: http://www.businessdictionary.com/definition/report.html
2. To provide information.
Read more: http://www.businessdictionary.com/definition/report.html
What are the benefits of the above experiments?
BalasHapusOne of the primary methods used to characterize a new compound is the physical determination of its normal melting and boiling points. The “normal” melting and boiling point is the temperature at which a substance melts or boils when the barometric pressure is 760 mmHg or 1 atm.
HapusWhy sometimes when we do it in laboratory ,the melting point or boiling point at thermometer its false ?
BalasHapusSuch things can be caused by internal or external factors, one of which the observer's inability to do so
HapusHow do we know the melting point of unknown substances from the experiment?
BalasHapusThe minimum required temperature of a solid-shaped substance to change its form to a liquid is called a melting point."
HapusTo know the melting point of a substance can use the following formula:
Q = m × L "
Information:
Q = the amount of heat needed to melt the substance, the unit joule (J)
M = mass of fusible substances, units of kilograms (kg)
L = heat melting substance, unit joule / kg (J / kg)
What compounds have high melting point?
BalasHapusThe bigger Mr. the higher the boiling point. And the highest boiling pointn-is pentane (C5H12) ,Mr = 72
Hapuscan you explain about primary methods used to characterize a new compound is the physical determination of its normal melting and boiling points? thanks
BalasHapusOne of the primary methods used to characterize a new compound is the physical determination of its normal melting and boiling points.The “normal” melting and boiling point is the temperature at which a substance melts or boils when the barometric pressure is 760 mmHg or 1 atm.
Hapus